Viscosity grading can be carried out on original (as-supplied) asphalt binder samples, referred to as AC grading, or on aged residue samples, known as AR grading. The AR viscosity test measures the viscosity of aged residue obtained from the rolling thin film oven test. AC grading characterizes asphalt binder properties before it undergoes the hot mix asphalt (HMA) manufacturing process. In contrast, the AR grading system aims to replicate asphalt binder properties after it has undergone a typical HMA manufacturing process, making it more representative of how asphalt binder behaves in HMA pavements. Table 1 provides an overview of the key advantages and disadvantages of the viscosity grading system.

Advantages and Disadvantages of Viscosity Grading:

Advantages:

  1. Represents Post-Manufacturing Behavior: AR grading better represents how asphalt binder behaves in HMA pavements, as it simulates post-manufacturing conditions.
  2. Realistic Performance Assessment: It provides a more realistic assessment of binder performance in the actual pavement environment.
  3. Better Aging Simulation: AR grading accounts for the aging effects that occur during the HMA manufacturing process.
  4. Improved Pavement Durability: Using AR grading can lead to better pavement durability predictions.

Disadvantages:

  1. Complex Testing: AR grading involves more complex testing procedures compared to AC grading.
  2. Limited Historical Data: There may be limited historical data available for AR-graded binders.
  3. Variability: Variability in the manufacturing process can affect the accuracy of AR grading results.
  4. Higher Costs: AR grading may involve higher testing costs compared to AC grading.

Please note that the advantages and disadvantages mentioned here are for informational purposes and may vary depending on specific applications and circumstances.

Advantages Disadvantages
Unlike penetration depth, viscosity serves as a fundamental engineering parameter At 25°C (77°F), the main grading may not accurately represent the rheological behavior of asphalt binders at low temperatures
Test temperatures are in alignment with key pavement temperature benchmarks: 25°C (77°F) for average pavement conditions, 60°C (140°F) for high pavement temperatures, and 135°C (275°F) for HMA mixing temperatures. In the AC grading system, the viscosities of thin film oven test residues within the same AC grade can exhibit substantial variations, leading to divergent post-construction performance among asphalt binders of the same grade.
The impact of temperature on asphalt binder rheology, known as temperature susceptibility, can be partially assessed through viscosity measurements carried out at three different temperature levels. (It’s worth mentioning that penetration measurements are exclusively conducted at 25°C or 77°F.) Viscosity testing is not only a lengthier process but also incurs higher costs in comparison to the penetration test.
Testing equipment and standards are easily accessible and widely available.

The new product grading method is now based on bitumen viscosity at 60°C and 135°C. This has led to the development of new grades with the following nomenclature:

Standard Grading Using Original Asphalt (AC): Grading Using Aged Residue (AR):
AASHTO M 226 AC-2.5 AC-5 AC-10 AC-20 AC-30 AC-40 AR-10 AR-20 AR-40 AR-80 AR-160
ASTM D 3381 AC-2.5 AC-5 AC-10 AC-20 AC-30 AC-40 AR-1000 AR-2000 AR-4000 AR-8000 AR-16000
Standard Minimum Absolute Grades Viscosity at 600°C, Poise Approximate Penetration Grade
IS73:2013 VG 10 800 80-100
VG 20 1600
VG 30 2400 60-70
VG 40 3200 30-40/40-50

Viscosity Grade vs. Penetration Grade: Addressing Key Issues

The transition from penetration grade to viscosity grade bitumen specifications has tackled several significant issues:

  1. Performance at High Temperatures: The adoption of viscosity-graded bitumen, determined by viscosity at 60°C rather than penetration at 25°C, addresses performance concerns at elevated temperatures. This shift is crucial for ensuring the durability of asphalt in hot climates.
  2. Compaction Challenges: Compaction issues caused by tender asphalt mixtures under roller wheels have been mitigated by introducing a minimum viscosity requirement at 135°C. This adjustment aims to minimize problems encountered during field applications.
  3. Reduced Testing Burden: The adoption of viscosity-graded paving bitumen specifications streamlines the testing process, reducing the total number of required tests to seven. This streamlining enhances efficiency without compromising bitumen quality or necessitating additional tests.

Viscosity-graded bitumen is classified based on its degree of fluidity, with higher grades indicating greater stiffness. These grades are determined through viscosity tests conducted at 60°C and 135°C, representing road surface and mixing temperatures during summer, respectively. Additionally, the penetration test at 25°C, reflecting the annual average pavement temperature, remains a part of the specifications.

By transitioning to viscosity grading, these specifications offer a more robust framework for assessing bitumen quality and performance in diverse environmental conditions.

Viscosity Grade Bitumen Specification (ASTM D3381-09)

The Viscosity Grade Bitumen Specification, as defined by ASTM D3381-09, is a crucial standard in the bitumen industry. This specification outlines the criteria for classifying bitumen based on its viscosity properties at elevated temperatures, specifically at 60°C and 135°C. These temperature points are representative of the conditions bitumen experiences during road construction and asphalt mixing processes.

By defining bitumen grades through viscosity measurements, this specification offers a more accurate representation of how bitumen will perform under varying environmental and operational conditions. This is especially significant in regions with extreme temperature fluctuations, as it ensures the asphalt’s long-term durability and performance.

The adoption of Viscosity Grade Bitumen Specifications, as outlined in ASTM D3381-09, is a pivotal step in modernizing the bitumen industry. It allows for more precise quality control and paves the way for improved asphalt formulations, ultimately leading to better road infrastructure and increased safety for motorists.

Property Units AC-10 AC-20 AC-30 AC-40 Test Methods
Viscosity, 140°F (60°C) P 1000±200 2000±400 3000±600 4000±800 ASTM D-2171
Viscosity, 275°F (135°C), Min cSt 150 210 250 300 ASTM D-2171
Penetration, 77°F (25°C), 100g, 5sec, Min 0.1MM 70 40 30 20 ASTM D-5
Flash point, Cleveland open cup, Min °C 219 232 232 232 ASTM D-92
Solubility in trichloroethylene, Min %Wt 99 99 99 99 ASTM D-2042
Tests on residue from thin-film oven test:
  – Viscosity, 140°F (60°C), Max P 5,000 10,000 15,000 20,000 ASTM D-2171
  – Ductility, 77°F (25°C), 5cm/min, Min CM 50 20 15 10 ASTM D-113

Viscosity Grade Bitumen Specification (IS 73:2013)

The Viscosity Grade Bitumen Specification, as defined by IS 73:2013, plays a pivotal role in the bitumen industry. This specification sets forth the criteria for classifying bitumen based on its viscosity properties at elevated temperatures, specifically at 60°C and 135°C. These temperature benchmarks closely mirror the conditions that bitumen encounters during road construction and asphalt mixing processes.

By categorizing bitumen grades using viscosity measurements, this specification offers a more accurate depiction of how bitumen will perform under diverse environmental and operational circumstances. This is particularly valuable in regions characterized by extreme temperature variations, ensuring the longevity and performance of asphalt pavements.

The adoption of Viscosity Grade Bitumen Specifications, as outlined in IS 73:2013, represents a significant advancement in the bitumen sector. It enables precise quality control, fostering enhanced asphalt formulations, ultimately leading to superior road infrastructure and heightened safety for road users.

Property Units VG-10 VG-20 VG-30 VG-40 Test Methods
Penetration at 25°C, 100g, 5sec, Min 0.1MM 80 60 45 35 IS 1203
Absolute viscosity at 60°C P 800-1200 1600-2400 2400-3600 3200-4800 IS 1206 (Part 2)
Kinematic viscosity at 135°C, Min cSt 250 300 350 400 IS 1206 (Part 3)
Flash point (Cleveland open cup), Min °C 220 220 220 220 IS 1448 [P : 69]
Solubility in trichloroethylene, Min %Wt 99 99 99 99 IS 1216
Softening point (R&B), Min °C 40 45 47 50 IS 1205
Tests on residue from thin film oven test:
  – Viscosity ratio at 60°C, Max 4 4 4 4 IS 1206 (Part 2)
  – Ductility at 25°C, Min CM 75 50 40 25 IS 1208